C₂₆H₃₆O₅

Base Information

Chemical Name:C₂₆H₃₆O₅
CAS No.:1372122-77-4
Molecular Formula:C₂₆H₃₆O₅
Molecular Weight:428.569
Hs Code.:

C<sub>26</sub>H<sub>36</sub>O<sub>5</sub>

Synonyms:C₂₆H₃₆O₅

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Chemical Property of C₂₆H₃₆O₅

Chemical Property:

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Technology Process of C₂₆H₃₆O₅

There total 9 articles about C₂₆H₃₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₄₂O₄S₂

: 1372122-77-4
C₂₆H₃₆O₅

Guidance literature:: With 2,6-dimethylpyridine; mercury(II) perchlorate tetrahydrate; water; calcium carbonate; In tetrahydrofuran; at 0 ℃; for 0.00555556h;
DOI:10.1021/ol3007259

Reference yield:

: 1372122-72-9
C₂₃H₃₁NO₂S₂

: 1372122-77-4
C₂₆H₃₆O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanol; lithium borohydride / diethyl ether / 0 - 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 40 °C / Inert atmosphere

3.1: osmium(VIII) oxide; N,N,N,N,-tetramethylethylenediamine / dichloromethane / 14 h / -78 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere

5.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve

6.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere

6.2: -78 °C / Inert atmosphere

7.1: 2,6-dimethylpyridine; mercury(II) perchlorate tetrahydrate; water; calcium carbonate / tetrahydrofuran / 0.01 h / 0 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; methanol; osmium(VIII) oxide; lithium borohydride; n-butyllithium; tetrapropylammonium perruthenate; mercury(II) perchlorate tetrahydrate; N,N,N,N,-tetramethylethylenediamine; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; calcium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; dichloromethane;
DOI:10.1021/ol3007259

Reference yield:

: 1372122-75-2
C₁₅H₂₂O₄

: 1372122-77-4
C₂₆H₃₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / dichloromethane / 12 h / Inert atmosphere

2.1: tetrapropylammonium perruthenate; 4-methylmorpholine N-oxide / dichloromethane / 3 h / Inert atmosphere; Molecular sieve

3.1: n-butyllithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 0.67 h / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine; mercury(II) perchlorate tetrahydrate; water; calcium carbonate / tetrahydrofuran / 0.01 h / 0 °C

With 2,6-dimethylpyridine; n-butyllithium; tetrapropylammonium perruthenate; mercury(II) perchlorate tetrahydrate; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; calcium carbonate; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/ol3007259