5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

Base Information

Chemical Name:5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose
CAS No.:899436-70-5
Molecular Formula:C₂₈H₂₈O₆
Molecular Weight:460.527
Hs Code.:

Synonyms:5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

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Chemical Property of 5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

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Technology Process of 5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

There total 4 articles about 5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65462-15-9
3-O-benzyl-1,2-O-isopropylidene-β-L-arabino-pentodialdo-1,4-furanose

: 899436-70-5
5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: periodic acid / toluene; tetrahydrofuran / 4.5 h / 0 °C / Inert atmosphere

2: pyridine / 18.5 h / 0 - 20 °C

With pyridine; periodic acid; In tetrahydrofuran; toluene;
DOI:10.1016/j.bmcl.2013.08.069

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 899436-70-5
5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: periodic acid / ethyl acetate / 1.5 h / 20 °C

2: periodic acid / toluene; tetrahydrofuran / 4.5 h / 0 °C / Inert atmosphere

3: pyridine / 18.5 h / 0 - 20 °C

With pyridine; periodic acid; In tetrahydrofuran; ethyl acetate; toluene;
DOI:10.1016/j.bmcl.2013.08.069

Reference yield:

: 18439-42-4,18439-43-5
3-O-benzyl-1,2-O-isopropylidene-5-C-phenyl-α-L-ido-pentofuranose

: 899436-70-5
5-O-benzoyl-3-O-benzyl-1,2-isopropylidene-5-C-phenyl-α-D-gluco-pentofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridinium chlorochromate / dichloromethane / 3 h / Reflux

2: L-Tartaric acid; sodium tetrahydroborate / tetrahydrofuran / 4.5 h / 0 - 20 °C

3: pyridine / 18.5 h / 0 - 20 °C

With pyridine; sodium tetrahydroborate; L-Tartaric acid; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2013.08.069