O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

Base Information

Chemical Name:O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat
CAS No.:1263776-14-2
Molecular Formula:C₁₉H₂₇NO₄S₄
Molecular Weight:461.692
Hs Code.:

Synonyms:O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

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Technology Process of O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

There total 1 articles about O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1101206-99-8
dithiocarbonic acid O-ethyl ester S-[4-oxo-1-(toluene-4-sulfonyl)-piperidin-3-yl]ester

: 627-50-9
vinyl ethylsulfide

: 1263776-14-2
O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

Guidance literature:: With dilauryl peroxide; In ethyl acetate; Reflux; Inert atmosphere;
DOI:10.1021/ol103044x

Reference yield: 62.0%

: 1263776-14-2
O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

: C₁₆H₂₁NO₃S₂

: C₁₆H₂₁NO₃S₂

: 1263776-33-5
(E)-3-(2-(ethylthio)ethylidene)-1-tosylpiperidin-4-one

Guidance literature:: In diphenylether; at 190 ℃; Inert atmosphere;
DOI:10.1021/ol103044x

Reference yield:

: 1263776-14-2
O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat

: 1263776-38-0
3-hydroxy-1-tosyl-3-vinylpiperidin-4-one

Guidance literature:: O-ethyl S-1-(ethylthio)-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl carbonodithioat; In diphenylether; at 190 ℃; Inert atmosphere;

With sodium periodate; In methanol; water; at 20 ℃; Inert atmosphere;

With triphenylphosphine; In toluene; Reflux; Inert atmosphere;
DOI:10.1021/ol103044x