1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion

Base Information

• Chemical Name: 1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion
• CAS No.: 71304-25-1
• Molecular Formula: C₂₀H₂₃N₃O₃
• Molecular Weight: 353.421

Synonyms:1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion

Chemical Property of 1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion

Chemical Property:

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Technology Process of 1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion

There total 1 articles about 1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5,10-trion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 2,3,4,5,6,6-hexamethylcyclohexa-2,4-dien-1-one (3854-96-4) → 1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5,10-trion (71304-25-1)

Guidance literature:

In benzene; for 12h; Heating;

Reference yield: 66.0%

1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5,10-trion (71304-25-1) → 2,3,3,4,5,6-Hexamethyl-9-phenyl-1,7,9-triazatricyclo<5.3.0.02,4>dec-5-en-8,10-dion (100084-77-3) + 1,2,8,9,9,11-Hexamethyl-5-phenyl-3,5,7-triazatetracyclo<6.3.0.02,11.03,7>undecan-4,6,10-trion (100084-76-2)

Guidance literature:

In acetone; for 12h; Irradiation;

Reference yield: 56.0%

1,7,8,9,11,11-Hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5,10-trion (71304-25-1) → (1S*,10R*)-10-Hydroxy-1,7,8,9,11,11-hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (100084-53-5) + (1S*,10S*)-10-Hydroxy-1,7,8,9,11,11-hexamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.02,6>undec-8-en-3,5-dion (100164-16-7)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 12h; 0 deg C to RT;

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

2,3,4,5,6,6-hexamethylcyclohexa-2,4-dien-1-one

Downstream raw materials:

(1S^*,10R^*)-10-Hydroxy-1,7,8,9,10,11,11-heptamethyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

(1R^*,10R^*)-10-Hydroxy-1,7,8,9,10,11,11-heptamethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

(1R^*,10S^*)-10-Hydroxy-1,7,8,9,10,11,11-heptamethyl-4-phenyl-2,4,6-triazatricyclo<5.3.1.0^2,6>undec-8-en-3,5-dion

(1R^*,10R^*)-10-Hydroxy-1,7,8,9,11,11-hexamethyl-103>methyl-4-phenyl-2,4,6-triazatricyclo<5.2.2.0^2,6>undec-8-en-3,5-dion

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