cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

Base Information

Chemical Name:cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide
CAS No.:1028318-05-9
Molecular Formula:C₂₁H₂₄N₄O
Molecular Weight:348.448
Hs Code.:

cycloheptanecarboxylic acid [4-(5-amino-1<i>H</i>-benzoimidazol-2-yl)-phenyl]-amide

Synonyms:cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

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Technology Process of cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

There total 4 articles about cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026982-71-7
cycloheptanecarboxylic acid [4-(5-nitro-1H-benzoimidazol-2-yl)-phenyl]-amide

: 1028318-05-9
cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; at 80 ℃; for 16h;
DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1028318-05-9
cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / polyphosphoric acid / xylene / 60 - 150 °C

2: pyridine / 3 h / 20 °C

3: H₂ / Pd/C / methanol; tetrahydrofuran / 16 h / 80 °C

With pyridine; PPA; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; xylene;
DOI:10.1016/j.ejmech.2006.03.014

Reference yield:

: 99-56-9
4-Nitrophenylene-1,2-diamine

: 1028318-05-9
cycloheptanecarboxylic acid [4-(5-amino-1H-benzoimidazol-2-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / polyphosphoric acid / xylene / 60 - 150 °C

2: pyridine / 3 h / 20 °C

3: H₂ / Pd/C / methanol; tetrahydrofuran / 16 h / 80 °C

With pyridine; PPA; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; xylene;
DOI:10.1016/j.ejmech.2006.03.014