2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

Base Information

Chemical Name:2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester
CAS No.:1311146-41-4
Molecular Formula:C₁₈H₁₇BrF₂O₂
Molecular Weight:383.233
Hs Code.:

Synonyms:2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

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Chemical Property of 2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

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Technology Process of 2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

There total 1 articles about 2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1311146-40-3
2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylcyclohexa-1,4-dienecarboxylic acid ethyl ester

: 1311146-41-4
2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 40 ℃; for 2h;
DOI:10.1016/j.tet.2011.03.073

Reference yield: 97.0%

: 1311146-41-4
2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

: 1311146-46-9
{2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylphenyl}methanol

Guidance literature:: 2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester; With lithium triethylborohydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

With hydrogenchloride; ammonium chloride; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2011.03.073

Reference yield: 82.0%

: 1311146-41-4
2-[(4-bromophenyl)difluoromethyl]-4,5-dimethylbenzoic acid ethyl ester

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1311146-45-8
2-[difluoro(4-vinylphenyl)methyl]-4,5-dimethylbenzoic acid ethyl ester

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 90 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2011.03.073