1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene

Base Information

• Chemical Name: 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene
• CAS No.: 109640-37-1
• Molecular Formula: C₂₉H₂₁F₇O
• Molecular Weight: 518.474

Synonyms:1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene

Chemical Property of 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene

Chemical Property:

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Technology Process of 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene

There total 21 articles about 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-((R)-1,2-Diphenyl-butyl)-phenol (6462-60-8,109640-34-8,109640-35-9) → 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-37-1) + 1-[4-((1R,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-36-0,109640-37-1)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 22 ℃; for 2h; Yield given;

DOI:10.1021/jm00393a014

Reference yield:

4-((R)-1,2-Diphenyl-butyl)-phenol (6462-60-8,109640-34-8,109640-35-9) → 1-[4-((1S,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-37-1) + 1-[4-((1R,2R)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-36-0,109640-37-1)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 22 ℃; for 2h; Yield given;

DOI:10.1021/jm00393a014

Reference yield:

perfluorotoluene (434-64-0) + 4-((S)-1,2-Diphenyl-butyl)-phenol (6462-60-8,109640-34-8,109640-35-9) → 1-[4-((1S,2S)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-36-0,109640-37-1) + 1-[4-((1R,2S)-1,2-Diphenyl-butyl)-phenoxy]-2,3,5,6-tetrafluoro-4-trifluoromethyl-benzene (109640-36-0)

Guidance literature:

With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In dichloromethane; at 22 ℃; for 2h; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jm00393a014

upstream raw materials:

perfluorotoluene

4-((S)-1,2-Diphenyl-butyl)-phenol

(2R)-2-phenylbutanoic acid

methoxybenzene

Downstream raw materials:

4-((1S,2R)-1,2-Diphenyl-butyl)-phenol

(1S,2R)-1-<4-<2-(dimethylamino)ethoxy>phenyl>-1,2-diphenylbutane

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