2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid

Base Information

• Chemical Name: 2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid
• CAS No.: 76086-49-2
• Molecular Formula: C₂₀H₃₀N₄O₄P₂S₂
• Molecular Weight: 516.562

Synonyms:2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid

Chemical Property of 2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid

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Technology Process of 2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid

There total 1 articles about 2.4.6.8-Tetraethyl-3.7-diphenyl-1λ⁶,5λ⁶-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

1,3-diethylsulfamide (6104-21-8) + Dichlorophenylphosphine (644-97-3) → 2.4.6.8-Tetraethyl-3.7-diphenyl-1λ6,5λ6-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid (76086-49-2)

Guidance literature:

With triethylamine; In diethyl ether; for 4h; Heating;

Reference yield: 93.0%

2.4.6.8-Tetraethyl-3.7-diphenyl-1λ6,5λ6-dithia-2.4.6.8-tetraaza-3.7-diphosphorocin-1.1.5.5.tetroxid (76086-49-2) → 1,3,5,7-Tetraethyl-4-phenyl-2,6-dithia-1,3,5,7-tetraaza-4λ5-phospha-spiro[3.3]heptane 2,2,6,6-tetraoxide

Guidance literature:

With phosphorus pentachloride; In tetrachloromethane; for 4h; Heating;

upstream raw materials:

1,3-diethylsulfamide

Dichlorophenylphosphine

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