(2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one

Base Information

• Chemical Name: (2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one
• CAS No.: 1173294-00-2
• Molecular Formula: C₂₁H₂₇BrO₄Si
• Molecular Weight: 451.432

Synonyms:(2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one

Chemical Property of (2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one

There total 1 articles about (2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C22H30O7SSi (1173293-90-7) → (2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one (1173294-00-2)

Guidance literature:

With lithium bromide; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1016/j.tetlet.2009.04.032

Reference yield:

(2S,3S,4S)-5-bromo-1-(methyldiphenylsilyl)-2,3,4-(trimethoxy)pentan-1-one (1173294-00-2) → C21H28O4Si (1173293-91-8) + C21H28O4Si

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 2h; optical yield given as %de;

DOI:10.1016/j.tetlet.2009.04.032

upstream raw materials:

C₂₂H₃₀O₇SSi

Downstream raw materials:

C₂₁H₂₈O₄Si

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