N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

Base Information

Chemical Name:N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester
CAS No.:67942-81-8
Molecular Formula:C₁₈H₁₅Cl₃NO₅P
Molecular Weight:462.654
Hs Code.:

Synonyms:N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

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Chemical Property of N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

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Technology Process of N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

There total 3 articles about N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 67942-80-7,88691-00-3,88691-01-4
N-phthalyl-1-amino-1-phenylmethanephosphonic acid 2,2,2-trichloroethyl monoester

: 67942-81-8
N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

Guidance literature:: In methanol; diethyl ether;

Reference yield:

: 59191-44-5
N-phthaloyl-1-aminophenylphosphonic acid

: 67942-81-8
N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / trichloroacetonitrile / pyridine / 6 h / 100 °C

2: 92 percent / methanol; diethyl ether

With trichloroacetonitrile; In pyridine; methanol; diethyl ether;

Reference yield:

: 67942-82-9
N-phthalyl-1-amino-1-phenylmethanephosphonic acid ethyl-2,2,2-trichloroethyl diester

: 67942-81-8
N-phthalyl-1-amino-1-phenylmethanephosphonic acid methyl-2,2,2-trichloroethyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 45percent HBr / acetic acid / 6 h / Ambient temperature

2: 92 percent / methanol; diethyl ether

With hydrogen bromide; In methanol; diethyl ether; acetic acid;