pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

Base Information

Chemical Name:pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾
CAS No.:108417-88-5
Molecular Formula:C₁₈H₁₅NO₆W
Molecular Weight:525.17
Hs Code.:

pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten<sup>(0)</sup>

Synonyms:pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

There total 2 articles about pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (ethoxyphenylcarbene)pentacarbonyltungsten⁽⁰⁾

: 2835-21-4
allyl isocyanide

: 108417-88-5
pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

Guidance literature:: In Petroleum ether; dropwise addn. of isocyanide soln. to W-compd. under inert gas, stirring at 0°C; removing solvent at 20°C, 15 Torr, elem. anal.;

Reference yield: 39.0%

: 108417-90-9
pentacarbonyl[2,2-diethoxy-2-phenyl-1-(2-propenylamino)ethylidene]tungsten⁽⁰⁾

: 14040-11-0
tungsten hexacarbonyl

: 108451-15-6
(CO)4WC(NHCH₂CHCH₂)C(O)(C₆H₅)

: 108417-88-5
pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

: 108451-14-5
(CO)4WC(NHCH₂CHCH₂)C(OC₂H₅)2(C₆H₅)

: 108451-17-8
2-ethoxy-2-phenyl-4-pentenenitrile

Guidance literature:: In toluene; heating of W-complex for 6 h at 80°C under inert gas; crystn. of W(CO)6 at 0°C, decantation, chromy. on silica gel (petroleum ether/ether), monitored by (1)H-NMR;

Reference yield: 74.0%

: 108417-88-5
pentacarbonyl(2-ethoxy-2-phenyl-4-pentenenitrile-N)tungsten⁽⁰⁾

: 14586-49-3
(pyridine)pentacarbonyltungsten⁽⁰⁾

: 108451-17-8
2-ethoxy-2-phenyl-4-pentenenitrile

Guidance literature:: With pyridine; In Petroleum ether; addn. of pyridine to W-compound, warming to 40°C for 40 min under inert gas; crystn. of W-complex at 0°C, decantation and chromy. on silica gel (petroleum ether) gives pentenenitrile and residue of W-compound, elem. anal. of pentenenitrile;