1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

Base Information

Chemical Name:1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide
CAS No.:1335100-34-9
Molecular Formula:C₁₅H₂₁NO₄S
Molecular Weight:311.402
Hs Code.:

Synonyms:1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

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Chemical Property of 1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

Chemical Property:

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Technology Process of 1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

There total 6 articles about 1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1262760-00-8
(S)-1-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)cyclopropane-1-sulfonyl chloride

: 62-53-3
aniline

: 1335100-34-9
1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

Guidance literature:: With pyridine; lithium bromide; In dichloromethane; at 20 ℃;

Reference yield:

: 1262760-34-8
sodium (S)-1-((2,2-dimethyl-1,3-dioxolan-4-yl)methyl)cyclopropane-1-sulfonate

: 1335100-34-9
1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; trichlorophosphate / 20 °C

2: pyridine; lithium bromide / dichloromethane / 20 °C

With pyridine; lithium bromide; trichlorophosphate; In dichloromethane;

Reference yield:

: 1335100-23-6
butyl 1-[(2S)-3-{[tert-butyl(dimethyl)silyl]oxy}-2-hydroxypropyl]cyclopropanesulfonate

: 1335100-34-9
1-{[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]methyl}-N-phenylcyclopropanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / water; methanol / 1 h

2: pyridinium p-toluenesulfonate / tetrahydrofuran

3: sodium methylate / 1,2-dimethoxyethane; methanol / 1.5 h / Reflux

4: pyridine; trichlorophosphate / 20 °C

5: pyridine; lithium bromide / dichloromethane / 20 °C

With pyridine; hydrogenchloride; sodium methylate; pyridinium p-toluenesulfonate; lithium bromide; trichlorophosphate; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water;