Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4

Base Information

• Chemical Name: Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4
• CAS No.: 1023697-62-2
• Molecular Formula: C₄₈H₇₆N₈Sb₄
• Molecular Weight: 1252.19

Synonyms:Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4

Chemical Property of Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4

There total 2 articles about Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

Sb(C6H3-2,6-(CH2NMe2)2)Cl2 (144501-67-7) → Sb4(C6H3-2,6-(CH2NMe2)2)4 (1023697-62-2)

Guidance literature:

With K[B(isobutyl)3H]; In tetrahydrofuran; byproducts: hydrogen; addn. of soln. of K(B(i-Bu)3H) (2 equiv.) in THF to precooled (0°C) soln. of SbCl2(C6H3(CH2NMe2)2) in THF; warming to room temp.; stirring for 24; evolution of H2; evapn. of solvent in vac., extn. with hexane; filtration, concn.; crystn. for 5 h at 0°C; filtration, washing with hexane; elem. anal.;

DOI:10.1021/om800227m

Reference yield: 20.0%

Sb(C6H3-2,6-(CH2NMe2)2)Cl2 (144501-67-7) → Sb5(C6H3-2,6-(CH2NMe2)2)3 (1024021-17-7) + Sb4(C6H3-2,6-(CH2NMe2)2)4 (1023697-62-2)

Guidance literature:

With K[B(isobutyl)3H]; In tetrahydrofuran; byproducts: hydrogen, C6H4(CH2N(CH3)2)2; addn. of soln. of K(B(i-Bu)3H) (2 equiv.) in THF to precooled (0°C) soln. of SbCl2(C6H3(CH2NMe2)2) in THF; warming to room temp.; stirring for 10 min; evolution of H2; evapn. of solvent in vac., extn. with hexane; filtration, concn.; crystn. for 5 h; filtration, washing with hexane;

DOI:10.1021/om800227m

upstream raw materials:

Sb(C₆H₃-2,6-(CH₂NMe₂)2)Cl₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1023697-62-2 Sb₄(C₆H₃-2,6-(CH₂NMe₂)2)4

Send

Send

Metric Ton KG G Pound L ML

Send

Send