N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Base Information

Chemical Name:N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine
CAS No.:1453118-05-2
Molecular Formula:C₃₀H₃₉ClN₂O₁₃
Molecular Weight:671.098
Hs Code.:

Synonyms:N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

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Chemical Property of N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

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Technology Process of N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

There total 2 articles about N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6304-89-8
3-acetoxybenzoic acid

: C₂₁H₃₃ClN₂O₁₀

: 1453118-05-2
N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h; Inert atmosphere;
DOI:10.1002/ejoc.201300236

Reference yield:

: 1453118-01-8
N-[(1R,2S,4S,5S)-2-(benzyloxycarbonylamino)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

: 1453118-05-2
N-[(1R,2S,4S,5S)-2-(3-acetoxybenzamido)-4-(2-chloroethoxy)-5-hydroxycyclohexane]-2,3,4-tri-O-acetyl-α-L-fucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol; N,N-dimethyl-formamide / 20 °C / 750.08 Torr / Inert atmosphere

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 15 h / 20 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201300236