1,4-cubanedicarboxilic acid dihydrazide

Base Information

• Chemical Name: 1,4-cubanedicarboxilic acid dihydrazide
• CAS No.: 325814-26-4
• Molecular Formula: C₁₀H₁₂N₄O₂
• Molecular Weight: 220.231

Synonyms:1,4-cubanedicarboxilic acid dihydrazide

Chemical Property of 1,4-cubanedicarboxilic acid dihydrazide

Chemical Property:

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Technology Process of 1,4-cubanedicarboxilic acid dihydrazide

There total 1 articles about 1,4-cubanedicarboxilic acid dihydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

cubane-1,4-dicarboxylic acid dimethyl ester (29412-62-2) → 1,4-cubanedicarboxilic acid dihydrazide (325814-26-4)

Guidance literature:

With hydrazine hydrate; In ethanol; for 8h; Heating;

DOI:10.1007/BF02495176

Reference yield: 92.0%

4-nitrobenzaldehdye (555-16-8) + 1,4-cubanedicarboxilic acid dihydrazide (325814-26-4) → 1,4-bis[4'-(4''-nitrophenyl)-1'-oxo-2',3'-diazabut-3'-en-1'-yl]cubane

Guidance literature:

In ethanol; acetic acid; for 1h;

DOI:10.1007/BF02495176

Reference yield: 89.0%

4-dimethylamino-benzaldehyde (100-10-7) + 1,4-cubanedicarboxilic acid dihydrazide (325814-26-4) → 1,4-bis[4'-(4''-dimethylaminophenyl)-1'-oxo-2',3'-diazabut-3'-en-1'-yl]cubane

Guidance literature:

In ethanol; acetic acid; for 1h;

DOI:10.1007/BF02495176

upstream raw materials:

cubane-1,4-dicarboxylic acid dimethyl ester

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