3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

Base Information

Chemical Name:3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene
CAS No.:158667-53-9
Molecular Formula:C₂₅H₂₂N₆O₂
Molecular Weight:438.489
Hs Code.:

Synonyms:3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

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Chemical Property of 3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

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Technology Process of 3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

There total 2 articles about 3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 57508-53-9
3-nitrobenzenecarboximidic acid ethyl ester monohydrochloride

: 54998-26-4
2-amino-4-<5'-(piperidin-1''-yl)benzimidazol-2'-yl>aniline

: 158667-53-9
3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

Guidance literature:: With acetic acid; Heating;

Reference yield:

: 619-24-9
3-nitrobenzonitrile

: 158667-53-9
3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / HCl / ethanol

2: 77 percent / glacial AcOH / Heating

With hydrogenchloride; acetic acid; In ethanol;

Reference yield: 85.0%

: 158667-53-9
3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene

: 158667-57-3
3-amino-1-{5'-[5''-(piperidin-1'''-yl)-1H-benzimidazol-2''-yl]-3H-benzimidazol-2'-yl}benzene

Guidance literature:: 3-nitro-1-<5'-<5''-(piperidin-1'''-yl)benzimidazol-2''-yl>benzimidazol-2'-yl>benzene; With hydrogen; acetic acid; 5%-palladium/activated carbon; In methanol; at 20 ℃; for 24h; under 760.051 Torr;

With ammonia;