Technology Process of C26H30F3N5O7
There total 11 articles about C26H30F3N5O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
ethanol; water;
at 0 ℃;
for 1h;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: potassium carbonate / methanol / 0.17 h / 20 °C
1.2: 2 h / 20 °C
2.1: copper(II) sulfate; sodium L-ascorbate / methanol; water
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C
4.1: lithium perchlorate / acetonitrile / 20 h / 70 °C
5.1: triethylamine / dichloromethane / 20 h
6.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h
7.1: triethylamine / dichloromethane / 20 h
8.1: potassium hydroxide / tetrahydrofuran / 0.25 h / 0 °C
9.1: hydrogenchloride / ethanol; water / 1 h / 0 °C
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; lithium perchlorate; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja2104679
- Guidance literature:
-
Multi-step reaction with 8 steps
1: copper(II) sulfate; sodium L-ascorbate / methanol; water
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 h / 0 - 4 °C
3: lithium perchlorate / acetonitrile / 20 h / 70 °C
4: triethylamine / dichloromethane / 20 h
5: palladium 10% on activated carbon; hydrogen / methanol / 5 h
6: triethylamine / dichloromethane / 20 h
7: potassium hydroxide / tetrahydrofuran / 0.25 h / 0 °C
8: hydrogenchloride / ethanol; water / 1 h / 0 °C
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; lithium perchlorate; copper(II) sulfate; sodium L-ascorbate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1021/ja2104679