N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

Base Information

Chemical Name:N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester
CAS No.:261712-31-6
Molecular Formula:C₁₄H₁₅N₃O₅S
Molecular Weight:337.356
Hs Code.:

<i>N</i>-(5-<i>tert</i>-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

Synonyms:N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

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Chemical Property of N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

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Technology Process of N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

There total 4 articles about N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5781-53-3
monomethyl oxalyl chloride

: 261712-05-4
5-tert-Butyl-2-nitro-4-thiocyanato-phenylamine

: 261712-31-6
N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

Guidance literature:: With pyridine; at 20 ℃; for 16h;
DOI:10.1021/ol0056170

Reference yield:

: 5369-19-7
3-tert-butylaniline

: 261712-31-6
N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: KNO₃ / 0 - 20 °C

2: aq. K₂CO₃ / methanol / 16 h / 20 °C

3: 90 percent / NaBr; Br₂ / 0 - 20 °C

4: 98 percent / pyridine / 16 h / 20 °C

With pyridine; bromine; potassium carbonate; potassium nitrate; sodium bromide; In methanol; 1: Nitration / 2: Hydrolysis / 3: thiocyanation / 4: Acylation;
DOI:10.1021/ol0056170

Reference yield:

: 261711-98-2
N-(5-tert-butyl-2-nitro-phenyl)-2,2,2-trifluoro-acetamide

: 261712-31-6
N-(5-tert-butyl-2-nitro-4-thiocyanato-phenyl)-oxalamic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. K₂CO₃ / methanol / 16 h / 20 °C

2: 90 percent / NaBr; Br₂ / 0 - 20 °C

3: 98 percent / pyridine / 16 h / 20 °C

With pyridine; bromine; potassium carbonate; sodium bromide; In methanol; 1: Hydrolysis / 2: thiocyanation / 3: Acylation;
DOI:10.1021/ol0056170