((C₆F₅NCH₂CH₂)2NCH₃)ReOCl

Base Information

• Chemical Name: ((C₆F₅NCH₂CH₂)2NCH₃)ReOCl
• CAS No.: 282726-79-8
• Molecular Formula: C₁₇H₁₁ClF₁₀N₃ORe
• Molecular Weight: 684.938
• Mol file: 282726-79-8.mol

Synonyms:((C₆F₅NCH₂CH₂)2NCH₃)ReOCl

Chemical Property of ((C₆F₅NCH₂CH₂)2NCH₃)ReOCl

Chemical Property:

Purity/Quality:

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Technology Process of ((C₆F₅NCH₂CH₂)2NCH₃)ReOCl

There total 2 articles about ((C₆F₅NCH₂CH₂)2NCH₃)ReOCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.6%

[ReOCl3(PPh3)2] + (C6F5NHCH2CH2)2NCH3 (282726-67-4) → ((C6F5NCH2CH2)2NCH3)ReOCl (282726-79-8)

Guidance literature:

With 2,6-lutidine; In ethanol; RE complex, ligand and 2,6-lutidine in EtOH were stirred for 5 days; ppt. was filtered and washed with Et2O;

DOI:10.1021/ic901434u

Reference yield:

[NEt4]2[ReOCl5] + (C6F5NHCH2CH2)2NCH3 (282726-67-4) → ((C6F5NCH2CH2)2NCH3)ReOCl (282726-79-8)

Guidance literature:

With NEt₃; In acetonitrile; 22 deg C, 30 min;

DOI:10.1021/om0001117

upstream raw materials:

(C₆F₅NHCH₂CH₂)2NCH₃