{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

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Chemical Name:{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine
CAS No.:886525-59-3
Molecular Formula:C₄₉H₆₂N₆O₆Si₂
Molecular Weight:887.239
Hs Code.:

{9-[4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-5-(<i>tert</i>-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9<i>H</i>-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

Synonyms:{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

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Chemical Property of {9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

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Technology Process of {9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

There total 1 articles about {9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 190506-33-3
3′,5′-O-bis(tert-butyldimethylsilyl)-O⁶-(p-nitrophenylethyl)-2′-deoxy-2-fluoroguanosine

: 438250-48-7
3-(pyren-1-yl)propylamine

: 886525-59-3
{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

Guidance literature:: With pyridine; at 20 ℃; for 72h;
DOI:10.1246/bcsj.79.312

Reference yield: 72.0%

: 886525-59-3
{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

: 886525-60-6
2-hydroxymethyl-5-[6-[2-(4-nitro-phenyl)-ethoxy]-2-(3-pyren-1-yl-propylamino)-purin-9-yl]-tetrahydro-furan-3-ol

Guidance literature:: With triethylamine trihydrofluoride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1246/bcsj.79.312

Reference yield:

: 886525-59-3
{9-[4-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-2-yl]-6-[2-(4-nitro-phenyl)-ethoxy]-9H-purin-2-yl}-(3-pyren-1-yl-propyl)-amine

: 886525-62-8
9-{5-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-yl}-2-(3-pyren-1-yl-propylamino)-1,9-dihydro-purin-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / triethylamine trihydrofluoride / tetrahydrofuran / 24 h / 20 °C

2: 31 percent / pyridine / 48 h / 20 °C

3: 61 percent / pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 18 h / 20 °C

With pyridine; triethylamine trihydrofluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1246/bcsj.79.312