(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

Base Information

Chemical Name:(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate
CAS No.:1257244-21-5
Molecular Formula:C₃₃H₃₁NO₇S₂
Molecular Weight:617.744
Hs Code.:

Synonyms:(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

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Chemical Property of (3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

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Technology Process of (3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

There total 2 articles about (3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₂₄O₇S₂

: 100-65-2
N-Phenylhydroxylamine

: 1257244-21-5
(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

Guidance literature:: In toluene; at 20 ℃; for 3h; optical yield given as %ee;
DOI:10.1039/c0cc01577f

Reference yield:

: 1257244-32-8
(E)-ethyl 3-(2-((S)-1-formyl-3,3-bis(phenylsulfonyl)propyl)phenyl)acrylate

: 100-65-2
N-Phenylhydroxylamine

: 1257244-21-5
(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

: ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

Guidance literature:: In toluene; at 20 ℃; for 3h; optical yield given as %ee;
DOI:10.1039/c0cc01577f

Reference yield: 98.0%

: 1257244-21-5
(3S,3aS,8S,8aR)-ethyl 8-(2,2-bis(phenylsulfonyl)ethyl)-1-phenyl-3,3a,8,8a-tetrahydro-1H-indeno[2,1-c]isoxazole-3-carboxylate

: 1257244-33-9
(S)-ethyl 2-((1S,2R,3S)-3-(2,2-bis(phenylsulfonyl)ethyl)-2-(phenylamino)-2,3-dihydro-1H-inden-1-yl)-2-hydroxyacetate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 22 ℃; optical yield given as %ee;
DOI:10.1039/c0cc01577f