Technology Process of C24H33BrFN5O3
There total 7 articles about C24H33BrFN5O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(1S,2S,3S,5R)-(+)-isopinocampheylamine;
With
diisobutylaluminium hydride;
In
tetrahydrofuran; toluene;
at 0 ℃;
for 2h;
C16H20BrNO5;
In
tetrahydrofuran; toluene;
for 2h;
With
Rochelle's salt;
In
tetrahydrofuran; water; toluene;
for 5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2
1.2: pH 7
2.1: calcium chloride / diethyl ether / 3 h / 20 °C
3.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation
3.2: 2 h
4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C
5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
5.2: 2 h
5.3: 5 h
With
titanium(IV) isopropylate; hydrogenchloride; methyl orange; diisobutylaluminium hydride; sodium cyanoborohydride; calcium chloride;
In
tetrahydrofuran; methanol; diethyl ether; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: calcium chloride / diethyl ether / 3 h / 20 °C
2.1: titanium(IV) isopropylate / tetrahydrofuran / 0.5 h / 140 °C / Microwave irradiation
2.2: 2 h
3.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 0 °C
4.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C
4.2: 2 h
4.3: 5 h
With
titanium(IV) isopropylate; hydrogenchloride; diisobutylaluminium hydride; calcium chloride;
In
tetrahydrofuran; diethyl ether; water; toluene;
