11-phenyl-11H-benzofluorene

Base Information

• Chemical Name: 11-phenyl-11H-benzofluorene
• CAS No.: 131544-01-9
• Molecular Formula: C₂₃H₁₆
• Molecular Weight: 292.38
• Mol file: 131544-01-9.mol

Synonyms:11-phenyl-11H-benzofluorene

Chemical Property of 11-phenyl-11H-benzofluorene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 11-phenyl-11H-benzofluorene

There total 4 articles about 11-phenyl-11H-benzofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

11-hydroxy-11-phenyl-11H-benzofluorene → 11-phenyl-11H-benzofluorene (131544-01-9)

Guidance literature:

With hydrogen iodide; In acetic acid; at 80 ℃; for 1h; Yield given;

DOI:10.1021/jo00003a031

Reference yield:

11H-Benzo[b]fluoren-11-one (3074-03-1) → 11-phenyl-11H-benzofluorene (131544-01-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.73 g / tetrahydrofuran / 16 h

2: HI / acetic acid / 1 h / 80 °C

With hydrogen iodide; In tetrahydrofuran; acetic acid;

DOI:10.1021/jo00003a031

Reference yield:

phenyllithium (591-51-5) → 11-phenyl-11H-benzofluorene (131544-01-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.73 g / tetrahydrofuran / 16 h

2: HI / acetic acid / 1 h / 80 °C

With hydrogen iodide; In tetrahydrofuran; acetic acid;

DOI:10.1021/jo00003a031

upstream raw materials:

11H-Benzo[b]fluoren-11-one

phenyllithium