menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Base Information

• Chemical Name: menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate
• CAS No.: 121144-99-8
• Molecular Formula: C₂₄H₃₃NO₃S
• Molecular Weight: 415.597

Synonyms:menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Chemical Property of menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

Chemical Property:

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Technology Process of menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

There total 1 articles about menthyl (1R,4S)-(+)-(S)_S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-3-<(S)S-2-pyridylsulphinyl>acrylate (105802-70-8,105880-25-9) + cyclohexa-1,3-diene (1165952-91-9) → menthyl (1R,4S)-(+)-(S)S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate (121144-99-8)

Guidance literature:

With zinc dibromide; In dichloromethane; for 96h; Ambient temperature;

Reference yield: 95.0%

menthyl (1R,4S)-(+)-(S)S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate (121144-99-8) → menthyl (1R,4S)-(+)-endo-3-(2-pyridylthio)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate (121133-39-9)

Guidance literature:

With titanium(III) chloride; In ethanol; for 0.333333h;

Reference yield: 85.0%

menthyl (1R,4S)-(+)-(S)S-endo-3-(2-pyridylsulfinyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate (121144-99-8) → menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate (121133-40-2)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 5h; Ambient temperature;

upstream raw materials:

(Z)-3-<(S)_S-2-pyridylsulphinyl>acrylate

cyclohexa-1,3-diene

Downstream raw materials:

menthyl (1R,4S)-(+)-endo-3-(2-pyridylthio)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

menthyl (1R,4S)-(-)-endo-3-(2-pyridylsulfonyl)bicyclo<2.2.2>oct-5-ene-endo-2-carboxylate

menthyl (1R,4S)-(-)-bicyclo<2.2.2>octa-2,5-diene-2-carboxylate

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