tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

Base Information

Chemical Name:tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate
CAS No.:130277-88-2
Molecular Formula:C₂₇H₃₈N₂O₁₀
Molecular Weight:550.606
Hs Code.:

Synonyms:tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

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Chemical Property of tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

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Technology Process of tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

There total 1 articles about tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130277-80-4,130324-70-8,130324-72-0,130324-73-1
tert-butyl (3aR,5R,6S,7R)-6-acetamido-5-acetoxy-7-<(4S,5R)-5-acetoxy-2-phenyl-1,3-dioxan-4-yl>-3,3a,4,5,6,7-hexahydropyrido<1,2-c><1,2,3>triazole-3a-carboxylate

: 130277-88-2
tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

Guidance literature:: With sulfuric acid; Yield given. Multistep reaction; THF, room temp., 4h;
DOI:10.1002/hlca.19900730422

Reference yield: 95.0%

: 130277-88-2
tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

: 130277-91-7
tert-butyl 5-acetamido-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;
DOI:10.1002/hlca.19900730422

Reference yield:

: 130277-88-2
tert-butyl 5-acetamido-4,8-di-O-acetyl-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C-(hydroxymethyl)-D-erythro-L-allo-nononate

: 130277-87-1
tert-butyl 5-acetamido-2-amino-2-N,6-anhydro-7,9-O-benzylidene-2,3,5-trideoxy-2-C,4-O-methylene-D-erythro-L-allo-nononate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOMe / methanol / 24 h / Ambient temperature

2: 82 percent / pyridinium hydrochloride / CH₂Cl₂ / 1 h

With sodium methylate; pyridine hydrochloride; In methanol; dichloromethane;
DOI:10.1002/hlca.19900730422