diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

Base Information

Chemical Name:diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane
CAS No.:741685-44-9
Molecular Formula:C₃₁H₂₇FNOP
Molecular Weight:479.534
Hs Code.:

Synonyms:diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

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Technology Process of diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

There total 3 articles about diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17154-34-6
(trimethylsilyl)diphenylphosphine

: 4-[3-(4-fluorophenyl)-1-phenyl-2-propynylidene]morpholinium trifluoromethanesulfonate

: 741685-44-9
diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

Guidance literature:: With lithium chloride; In tetrahydrofuran; at -78 - 20 ℃; for 12h;
DOI:10.1021/jo049586o

Reference yield:

: 1-(4-fluorophenyl)-3-morpholino-3-phenyl-2-propen-1-one

: 741685-44-9
diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 2 h / -78 - 20 °C

2: 11.55 g / 0.25 h / 180 °C / 0 Torr

3: LiCl / tetrahydrofuran / 12 h / -78 - 20 °C

With lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo049586o

Reference yield:

: 4-[3-(4-fluorophenyl)-1-phenyl-3-(trifluoromethylsulfonyloxy)-2-propenylidene]morpholinium triflate

: 741685-44-9
diphenyl[1-(4-fluorophenyl)-3-morpholino-3-phenyl-1,2-propadienyl]phosphane

Guidance literature:: Multi-step reaction with 2 steps

1: 11.55 g / 0.25 h / 180 °C / 0 Torr

2: LiCl / tetrahydrofuran / 12 h / -78 - 20 °C

With lithium chloride; In tetrahydrofuran;
DOI:10.1021/jo049586o