C₃₇H₃₆O₅

Base Information

Chemical Name:C₃₇H₃₆O₅
CAS No.:1332271-52-9
Molecular Formula:C₃₇H₃₆O₅
Molecular Weight:560.69
Hs Code.:

C<sub>37</sub>H<sub>36</sub>O<sub>5</sub>

Synonyms:C₃₇H₃₆O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₃₆O₅

Chemical Property:

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Technology Process of C₃₇H₃₆O₅

There total 8 articles about C₃₇H₃₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1332271-08-5
C₁₈H₂₂O₅

: 76-83-5
trityl chloride

: 1332271-52-9
C₃₇H₃₆O₅

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1308721-86-9
2-hydroxy-3-methyl-4,5-dimethoxybenzaldehyde

: 1332271-52-9
C₃₇H₃₆O₅

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 2.08 h / -78 - 0 °C / Inert atmosphere

2.2: 16.08 h / 20 °C / Inert atmosphere

3.1: AD-mix-β; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

With dmap; AD-mix-β; potassium tert-butylate; water; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1332271-51-8
C₁₈H₂₀O₃

: 1332271-52-9
C₃₇H₃₆O₅

Guidance literature:: Multi-step reaction with 2 steps

1: AD-mix-β; water / tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

With dmap; AD-mix-β; water; triethylamine; In dichloromethane; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094