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C27H28N2O10

Base Information
  • Chemical Name:C27H28N2O10
  • CAS No.:161391-11-3
  • Molecular Formula:C27H28N2O10
  • Molecular Weight:540.527
  • Hs Code.:
C<sub>27</sub>H<sub>28</sub>N<sub>2</sub>O<sub>10</sub>

Synonyms:C27H28N2O10

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Chemical Property of C27H28N2O10
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Technology Process of C27H28N2O10

There total 4 articles about C27H28N2O10 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Guidance literature:
With dmap; acetic anhydride; triethylamine; In dichloromethane; at 25 ℃; for 120h;
DOI:10.1016/S0040-4020(01)89281-4
Guidance literature:
Multi-step reaction with 3 steps
1: PPTS / CHCl3 / 16 h / Heating
2: 92 percent / t-butyl lithium / pentane; tetrahydrofuran / 0.1 h / -78 °C
3: 82 percent / triethylamine, DMAP, acetic anhydride / CH2Cl2 / 120 h / 25 °C
With dmap; tert.-butyl lithium; pyridinium p-toluenesulfonate; acetic anhydride; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; pentane;
DOI:10.1016/S0040-4020(01)89281-4
Guidance literature:
Multi-step reaction with 3 steps
1: PPTS / CHCl3 / 16 h / Heating
2: 92 percent / t-butyl lithium / pentane; tetrahydrofuran / 0.1 h / -78 °C
3: 82 percent / triethylamine, DMAP, acetic anhydride / CH2Cl2 / 120 h / 25 °C
With dmap; tert.-butyl lithium; pyridinium p-toluenesulfonate; acetic anhydride; triethylamine; In tetrahydrofuran; dichloromethane; chloroform; pentane;
DOI:10.1016/S0040-4020(01)89281-4
upstream raw materials:

3,4-dihydro-2H-pyran

C20H19NO10

Downstream raw materials:

C26H30N2O9

C26H28N2O9

C29H36N2O9Si

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