1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene

Base Information

• Chemical Name: 1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene
• CAS No.: 862591-89-7
• Molecular Formula: C₂₆H₂₈N₂
• Molecular Weight: 368.522

Synonyms:1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene

Chemical Property of 1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene

Chemical Property:

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Technology Process of 1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene

There total 1 articles about 1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H28N2 (862591-84-2) → 1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene (862591-89-7)

Guidance literature:

In 5,5-dimethyl-1,3-cyclohexadiene; for 2h; Reflux;

DOI:10.1016/j.tet.2008.11.057

Reference yield: 97.0%

1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene (862591-89-7) + allyl bromide (106-95-6) → 11-N-allyl-1,6-diphenyl-2,2,7,7-tetramethyl-11,12-diazatetracyclo[4.4.0.1(3,10).1(5,8)]dodeca-5(12),10-diene-11-ium bromide

Guidance literature:

In chloroform; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.057

Reference yield: 88.0%

1,1,4,4-tetramethyl-2,5-diphenyl-1,3,3a,4,6,6a-hexahydro-6b,6c-diaza-dicyclopenta[cd,gh]pentalene (862591-89-7) + iodomethylbenzene (620-05-3) → 11-N-benzyl-1,6-diphenyl-2,2,7,7-tetramethyl-11,12-diazatetracyclo[4.4.0.1(3,10).1(5,8)]dodeca-5(12),10-diene-11-ium

Guidance literature:

In chloroform; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.057

upstream raw materials:

C₂₆H₂₈N₂

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