(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

Base Information

Chemical Name:(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate
CAS No.:1192264-06-4
Molecular Formula:C₂₉H₄₄O₅Si
Molecular Weight:500.751
Hs Code.:

Synonyms:(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

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Chemical Property of (S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

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Technology Process of (S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

There total 2 articles about (S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1192264-05-3
(S)-1-(2,2-dimethyl-4-oxo-4H-1,3-dioxin-6-yl)-6-(triisopropylsilyloxy)heptane-2,4-dione

: 1192264-07-5
(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-hydroxypropyl)benzoate

: 137494-03-2
(S)-3-hydroxy-5-methoxybenzyl-2-methyl-1,3-dioxolane

: 1192264-06-4
(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

: 1192264-08-6
(S)-1-(3,5-dihydroxy-2-((2,4,6-trimethylbenzyloxy)carbonyl)phenyl)propan-2-yl 2,4-dihydroxy-6-((S)-2-(triisopropylsilyloxy)propyl)benzoate

Guidance literature:: (S)-1-(2,2-dimethyl-4-oxo-4H-1,3-dioxin-6-yl)-6-(triisopropylsilyloxy)heptane-2,4-dione; (S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-hydroxypropyl)benzoate; In toluene; at 110 ℃; Inert atmosphere;

With cesium acetate; In dichloromethane; isopropyl alcohol; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; isopropyl alcohol; Inert atmosphere;
DOI:10.1021/jo9015858

Reference yield:

: C₂₉H₄₆O₆Si

: 1192264-06-4
(S)-2,4,6-trimethylbenzyl 2,4-dihydroxy-6-(2-(triisopropylsilyloxy)propyl)benzoate

Guidance literature:: C₂₉H₄₆O₆Si; With cesium acetate; In dichloromethane; isopropyl alcohol; at 20 ℃; for 10h; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; isopropyl alcohol; for 3h; pH=2; Inert atmosphere;
DOI:10.1021/jo9015858