C₈H₉BrFNO₂

Base Information

Chemical Name:C₈H₉BrFNO₂
CAS No.:1009092-77-6
Molecular Formula:C₈H₉BrFNO₂
Molecular Weight:250.067
Hs Code.:

C<sub>8</sub>H<sub>9</sub>BrFNO<sub>2</sub>

Synonyms:C₈H₉BrFNO₂

Suppliers and Price of C₈H₉BrFNO₂

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Chemical Property of C₈H₉BrFNO₂

Chemical Property:

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Technology Process of C₈H₉BrFNO₂

There total 3 articles about C₈H₉BrFNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈H₇BrFNO₂

: 1009092-77-6
C₈H₉BrFNO₂

Guidance literature:: C₈H₇BrFNO₂; With hydrogenchloride; methyl orange; sodium cyanoborohydride; In tetrahydrofuran; methanol; water; for 3h; pH=2;

With sodium hydroxide; In tetrahydrofuran; methanol; water;

Reference yield:

: 3-bromo-6-fluoro-2-hydroxybenzaldehyde

: 1009092-77-6
C₈H₉BrFNO₂

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

2: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

3: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; potassium carbonate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 147460-41-1
2-bromo-5-fluorophenol

: 1009092-77-6
C₈H₉BrFNO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.17 h / 20 °C

1.2: 2 h / Heating / reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

3.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

4.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; potassium carbonate; triethylamine; magnesium chloride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;