Technology Process of C30H35NO3SiS2
There total 7 articles about C30H35NO3SiS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / PPh3; DIAD / tetrahydrofuran / 4 h / 25 °C
2: 77 percent / aq. H2O2 / (NH4)6Mo7O24*4H2O / ethanol
With
di-isopropyl azodicarboxylate; dihydrogen peroxide; triphenylphosphine;
ammonium heptamolybdate;
In
tetrahydrofuran; ethanol;
1: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2006.12.119
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 99 percent / imidazole / dimethylformamide
2: 93 percent / m-CPBA / CHCl3 / -30 - 0 °C
3: 86 percent / H5IO6 / tetrahydrofuran; diethyl ether / 1 h / 0 °C
4: 99 percent / NaBH4 / ethanol / 0 °C
5: 97 percent / PPh3; DIAD / tetrahydrofuran / 4 h / 25 °C
6: 77 percent / aq. H2O2 / (NH4)6Mo7O24*4H2O / ethanol
With
1H-imidazole; sodium tetrahydroborate; di-isopropyl azodicarboxylate; dihydrogen peroxide; periodic acid; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
ammonium heptamolybdate;
In
tetrahydrofuran; diethyl ether; ethanol; chloroform; N,N-dimethyl-formamide;
5: Mitsunobu reaction;
DOI:10.1016/j.tetlet.2006.12.119