methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

Base Information

Chemical Name:methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside
CAS No.:153184-64-6
Molecular Formula:C₂₅H₄₂O₇SSi₂
Molecular Weight:542.841
Hs Code.:

Synonyms:methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

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Chemical Property of methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

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Technology Process of methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

There total 3 articles about methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 153223-25-7
methyl 3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

: 1005-56-7
phenylcarbonochloridothioate

: 153184-64-6
methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

Guidance literature:: In pyridine; dichloromethane; Ambient temperature;
DOI:10.1135/cccc19932159

Reference yield:

: 18043-71-5
1,1,3,3-tetraisopropyldisiloxane

: 153184-64-6
methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) bromine / 1.) CCl₄, room temperature, 4 h, 2.) pyridine, room temperature, 4 h

2: 65 percent / pyridine; CH₂Cl₂ / Ambient temperature

With bromine; In pyridine; dichloromethane;
DOI:10.1135/cccc19932159

Reference yield:

: 13039-64-0
(2S,3R,4R)-2-(hydroxymethyl)-5-methoxytetrahydrofuran-3,4-diol

: 153184-64-6
methyl 2-O-(phenoxythiocarbonyl)-3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-α-L-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) bromine / 1.) CCl₄, room temperature, 4 h, 2.) pyridine, room temperature, 4 h

2: 65 percent / pyridine; CH₂Cl₂ / Ambient temperature

With bromine; In pyridine; dichloromethane;
DOI:10.1135/cccc19932159