C₁₉H₂₈OSi

Base Information

Chemical Name:C₁₉H₂₈OSi
CAS No.:1338347-17-3
Molecular Formula:C₁₉H₂₈OSi
Molecular Weight:300.516
Hs Code.:

Synonyms:C₁₉H₂₈OSi

Suppliers and Price of C₁₉H₂₈OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₉H₂₈OSi

Chemical Property:

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Technology Process of C₁₉H₂₈OSi

There total 5 articles about C₁₉H₂₈OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1338347-16-2
C₂₀H₃₂O₂Si

: 1338347-17-3
C₁₉H₂₈OSi

: 1338347-18-4
C₁₉H₂₈OSi

Guidance literature:: With oct-1-ene; platinum(II) chloride; In toluene; at 100 ℃; for 0.0833333h; under 760.051 Torr; Inert atmosphere;
DOI:10.1021/ol202649j

Reference yield:

: 920754-35-4
C₉H₂₀OSi

: 1338347-17-3
C₁₉H₂₈OSi

: 1338347-18-4
C₁₉H₂₈OSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 23 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -40 °C / Inert atmosphere

2.2: -40 - 0 °C / Inert atmosphere

2.3: -40 - 23 °C / Inert atmosphere

3.1: sodium periodate; silica gel / dichloromethane; water / 1 h / 23 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

5.1: ethyl vinyl ether; platinum(II) chloride / tetrahydrofuran / 8 h / 23 °C / 760.05 Torr / Inert atmosphere

With sodium periodate; n-butyllithium; silica gel; diisobutylaluminium hydride; ethyl vinyl ether; 3-chloro-benzenecarboperoxoic acid; platinum(II) chloride; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water;
DOI:10.1021/ol202649j

Reference yield:

: 1338347-53-7
C₁₄H₂₈O₂Si

: 1338347-17-3
C₁₉H₂₈OSi

: 1338347-18-4
C₁₉H₂₈OSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / methanol / 4 h / 23 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 23 °C / Inert atmosphere

3.1: n-butyllithium / diethyl ether; hexane / 0.5 h / -40 °C / Inert atmosphere

3.2: -40 - 0 °C / Inert atmosphere

3.3: -40 - 23 °C / Inert atmosphere

4.1: sodium periodate; silica gel / dichloromethane; water / 1 h / 23 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 0.42 h / -78 °C / Inert atmosphere

6.1: ethyl vinyl ether; platinum(II) chloride / tetrahydrofuran / 8 h / 23 °C / 760.05 Torr / Inert atmosphere

With sodium periodate; n-butyllithium; silica gel; diisobutylaluminium hydride; toluene-4-sulfonic acid; ethyl vinyl ether; 3-chloro-benzenecarboperoxoic acid; platinum(II) chloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water;
DOI:10.1021/ol202649j