2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

Base Information

Chemical Name:2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole
CAS No.:34654-43-8
Molecular Formula:C₁₇H₁₂N₄
Molecular Weight:272.309
Hs Code.:

Synonyms:2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

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Chemical Property of 2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

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Technology Process of 2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

There total 3 articles about 2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1670-14-0
benzamidine monohydrochloride

: 28912-93-8
1-naphthyldiazonium tetrafluoroborate

: 34654-43-8
2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

Guidance literature:: benzamidine monohydrochloride; 1-naphthyldiazonium tetrafluoroborate; With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 1h;

With iodine; potassium iodide; In dimethyl sulfoxide; at 20 ℃; for 1h;
DOI:10.1021/acs.orglett.5b03068

Reference yield: 60.0%

: 34654-43-8
2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

Guidance literature:: With di-μ-hydroxo-bis[(N,N,N'N'-tetramethylethylenediamine)copper(II)] chloride; oxygen; potassium carbonate; lithium chloride; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 134-32-7
1-amino-naphthalene

: 34654-43-8
2-(naphthalen-1-yl)-5-phenyl-2H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrafluoroboric acid; sodium nitrite / water / 0.5 h / 0 °C

2.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

2.2: 1 h / 20 °C

With tetrafluoroboric acid; potassium carbonate; sodium nitrite; In water; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.5b03068