N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

Base Information

Chemical Name:N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide
CAS No.:256496-40-9
Molecular Formula:C₁₈H₂₄Cl₂N₃OP
Molecular Weight:400.288
Hs Code.:

Synonyms:N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

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Technology Process of N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

There total 1 articles about N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 127-88-8
N,N-di(2-chloroethyl)amidophosphoric acid dichloride

: 100-46-9
benzylamine

: 256496-40-9
N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

Guidance literature:: In diethyl ether; at -70 - 20 ℃; for 142h;
DOI:10.1039/a903835c

Reference yield: 63.0%

: 256496-40-9
N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

: 256496-41-0
3-(2-chloroethyl)-2-oxo-2-benzylamino-1-benzyl-1,3,2λ⁵-diazaphospholidine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 48h;
DOI:10.1039/a903835c

Reference yield:

: 256496-40-9
N,N-bis(2-chloroethyl)-N',N-dibenzylphosphoric triamide

: 256496-38-5
1-oxo-2,8-dibenzyl-2,5,8-triaza-1λ⁵-phosphabicyclo[3.3.0]octane

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / t-BuOK / tetrahydrofuran / 48 h / 20 °C

2: 58 percent / NaH; Bu₄NHSO₄ / tetrahydrofuran / 45 h / 20 °C

With potassium tert-butylate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydride; In tetrahydrofuran; 1: Cyclization / 2: Cyclization;
DOI:10.1039/a903835c