N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

Base Information

Chemical Name:N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester
CAS No.:10342-52-6
Molecular Formula:C₂₂H₃₃N₃O₇
Molecular Weight:451.52
Hs Code.:

N<sup>α</sup>-Benzyloxycarbonyl-N<sup>ε</sup>-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

Synonyms:N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

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Technology Process of N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

There total 7 articles about N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2389-60-8
Z-Lys(Boc)-OH

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 10342-52-6
N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2010.06.024

Reference yield: 90.0%

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 2212-76-2
N^α-benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysine dicyclohexylamine salt

: 10342-52-6
N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 0 - 25 ℃;
DOI:10.1021/jo00170a015

Reference yield: 70.0%

: 2389-60-8
Z-Lys(Boc)-OH

: 616-34-2
methoxycarbonylmethylamine

: 10342-52-6
N^α-Benzyloxycarbonyl-N^ε-tert-butyloxycarbonyl-L-lysylglycine Methyl Ester

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1016/j.bmcl.2006.10.061