s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

Base Information

Chemical Name:s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester
CAS No.:1423012-51-4
Molecular Formula:C₂₀H₁₈N₄O₄S₂
Molecular Weight:442.519
Hs Code.:

Synonyms:s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

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Chemical Property of s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

Chemical Property:

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Technology Process of s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

There total 6 articles about s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₆N₆OS₂

: 1080-06-4
L-Tyr-OMe

: 1423012-51-4
s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

Guidance literature:: L-Tyr-OMe; With triethylamine; In ethyl acetate; at 0 ℃; for 0.333333h;

C₁₀H₆N₆OS₂; In ethyl acetate; at 20 ℃; for 24h; Cooling;
DOI:10.1016/j.ejmech.2012.10.033

Reference yield:

: 40527-73-9
ethyl S-triazolo[3,4-b]benzothiazol-3-ylthioacetate

: 1423012-51-4
s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / ethanol / 1 h / Reflux

2.1: hydrogenchloride; sodium nitrite / water; acetic acid / 0.5 h / -5 - 0 °C

3.1: triethylamine / ethyl acetate / 0.33 h / 0 °C

3.2: 24 h / 20 °C / Cooling

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; In ethanol; water; acetic acid; ethyl acetate;
DOI:10.1016/j.ejmech.2012.10.033

Reference yield:

: 40527-80-8
benzo[4,5]thiazolo[2,3-c][1,2,4]triazol-3-ylsulfanyl-acetic acid hydrazide

: 1423012-51-4
s-triazolo[3,4-b]benzothiazol-3-ylthioacetyl (L)-tyrosine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water; acetic acid / 0.5 h / -5 - 0 °C

2.1: triethylamine / ethyl acetate / 0.33 h / 0 °C

2.2: 24 h / 20 °C / Cooling

With hydrogenchloride; triethylamine; sodium nitrite; In water; acetic acid; ethyl acetate;
DOI:10.1016/j.ejmech.2012.10.033