3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Base Information

• Chemical Name: 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene
• CAS No.: 205643-54-5
• Molecular Formula: C₂₁H₁₆Cl₂N₂O
• Molecular Weight: 383.277

Synonyms:3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Chemical Property of 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

There total 3 articles about 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cycloheptatrienylidene-4-methyl-aniline (949-68-8) + 2,6-dichlorobenzonitrile N-oxide (2904-62-3) → 3-(2,6-dichloro-phenyl)-4-p-tolyl-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-57-8) + 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-54-5) + [3-(2,6-dichloro-phenyl)-3aH-cyclohepta[d]isoxazol-4-yl]-p-tolyl-amine + [3-(2,6-dichloro-phenyl)-8aH-cyclohepta[d]isoxazol-4-yl]-p-tolyl-amine

Guidance literature:

In cyclohexane; at 21 ℃; for 12h; Yield given; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.3987/com-97-s(n)76

Reference yield:

N-cycloheptatrienylidene-4-methyl-aniline (949-68-8) + 2,6-dichlorobenzonitrile N-oxide (2904-62-3) → 3-(2,6-dichloro-phenyl)-4-p-tolyl-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-57-8) + 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-54-5)

Guidance literature:

In methanol; for 1h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.3987/com-97-s(n)76

Reference yield:

3-(2,6-dichloro-phenyl)-4-p-tolyl-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-57-8) → 3-(2,6-dichloro-phenyl)-4-p-tolyl-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-54-5)

Guidance literature:

In benzene-d6; at 20 ℃; Product distribution; equilibrium reaction; other deuteriated solvents;

DOI:10.3987/com-97-s(n)76

upstream raw materials:

3-(2,6-dichloro-phenyl)-4-p-tolyl-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene

N-cycloheptatrienylidene-4-methyl-aniline

2,6-dichlorobenzonitrile N-oxide

Downstream raw materials:

Tropone

1,3-di-p-tolylurea

3-(2,6-dichloro-phenyl)-4-p-tolyl-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene

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