acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide]

Base Information

• Chemical Name: acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide]
• CAS No.: 681463-91-2
• Molecular Formula: C₂₀H₁₇N₃O₃
• Molecular Weight: 347.373
• Mol file: 681463-91-2.mol

Synonyms:acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide]

Chemical Property of acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide]

There total 2 articles about acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenyl-2-[4-(4-nitrophenyl)phenyl]diazene → acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide] (681463-91-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aq.-ethanolic ammonia; hydrogen sulfide

With ammonium hydroxide; hydrogen sulfide;

DOI:10.1002/hlca.19430260315

Reference yield:

N-(4'-nitro-biphenyl-4-yl)-N'-phenyl-hydrazine + acetic anhydride (108-24-7) → acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide] (681463-91-2)

Guidance literature:

DOI:10.1002/hlca.19430260315

Reference yield:

acetic acid-[N'-(4'-nitro-biphenyl-4-yl)-N-phenyl-hydrazide] (681463-91-2) → Acetanilid (103-84-4) + p,p'-diaminobiphenyl (92-87-5)

Guidance literature:

Hydrogenation;

DOI:10.1002/hlca.19430260315

upstream raw materials:

acetic anhydride

Downstream raw materials:

Acetanilid

p,p'-diaminobiphenyl