Technology Process of C52H76N2SSn
There total 4 articles about C52H76N2SSn which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-Bromosuccinimide / tetrahydrofuran / 3 h / 0 °C
2.1: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 48 h / 100 °C
3.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C
3.2: 20 °C
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium;
In
tetrahydrofuran; 1,4-dioxane; hexane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 48 h / 100 °C
2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C
2.2: 20 °C
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium;
In
tetrahydrofuran; 1,4-dioxane; hexane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: copper(l) iodide; N,N`-dimethylethylenediamine; potassium phosphate / toluene / 72 h / Reflux
2.1: N-Bromosuccinimide / tetrahydrofuran / 3 h / 0 °C
3.1: tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / 48 h / 100 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C
4.2: 20 °C
With
potassium phosphate; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; N,N`-dimethylethylenediamine;
In
tetrahydrofuran; 1,4-dioxane; hexane; toluene;