N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide

Base Information

• Chemical Name: N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide
• CAS No.: 71316-14-8
• Molecular Formula: C₃₂H₂₇N₂P
• Molecular Weight: 470.554
• Mol file: 71316-14-8.mol

Synonyms:N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide

Chemical Property of N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide

There total 3 articles about N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-chloro-N'-p-tolylbenzamidine (66275-61-4) + triphenylphosphine (603-35-0) → C32H27N2P (71316-14-8)

Guidance literature:

With triethylamine; In benzene; at 20 ℃; for 3h;

Reference yield:

N-Chloro-N'-(4-methylphenyl)benzamidine (66275-61-4) + triphenylphosphine (603-35-0) → N'-(4-methylphenyl)-N-(triphenylphosphoranylidene)-benzenecarboximidamide (71316-14-8)

Guidance literature:

With sodium hydroxide; Yield given. Multistep reaction; 1) CH₂Cl₂, -50 deg C, 10 min;

DOI:10.1016/S0040-4039(00)94659-8

Reference yield:

→ C32H27N2P (71316-14-8)

Guidance literature:

N-p-Tolyl-N'-chlorbenzamidin, (C6H5)3P, KOH;

DOI:10.1246/bcsj.52.1541

upstream raw materials:

N-chloro-N'-p-tolylbenzamidine

triphenylphosphine

N-Chloro-N'-(4-methylphenyl)benzamidine

Downstream raw materials:

6-Methyl-4-phenethyl-2-phenyl-quinazoline

6-Methyl-4-phenethyl-2-phenyl-3,4-dihydro-quinazoline

6-Methyl-2-phenyl-4-(4-trifluoromethyl-phenyl)-quinazoline

6-Methyl-2-phenyl-4-(4-trifluoromethyl-phenyl)-3,4-dihydro-quinazoline