ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate

Base Information

• Chemical Name: ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate
• CAS No.: 1010396-22-1
• Molecular Formula: C₁₅H₁₆N₂O₇S
• Molecular Weight: 368.367
• Mol file: 1010396-22-1.mol

Synonyms:ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate

Chemical Property of ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate

There total 1 articles about ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

ethyl 2-hydroxy-2-hydroxymethyl-5-(2'-nitrobenzenesulfonamido)-cyclohex-3-enecarboxylate → ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate (1010396-22-1)

Guidance literature:

With sodium periodate; In tetrahydrofuran; water; at 0 ℃; for 3h;

DOI:10.1021/ol7029646

Reference yield:

ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate (1010396-22-1) → C15H16N2O6S (1010396-24-3)

Guidance literature:

ethyl 5-(2'-nitrobenzenesulfonamido)-2-oxocyclohex-3-enecarboxylate; With sodium tetrahydroborate; cerium(III) chloride; In methanol; at 0 ℃; for 2h;

With dmap; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 4h;

DOI:10.1021/ol7029646

Downstream raw materials:

C₁₅H₁₆N₂O₆S