Technology Process of PEt-3IB
There total 7 articles about PEt-3IB which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H31N3O3;
With
water; sodium hydroxide;
In
ethanol;
at 60 ℃;
for 1h;
With
hydrogenchloride; water;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h
2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol / 1 h / 20 °C
3.1: potassium carbonate / N,N-dimethyl-formamide / 17 h / 120 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
4.2: 0.17 h / 20 °C
5.1: water; sodium hydroxide / ethanol / 1 h / 60 °C
With
hydrogenchloride; water; hydrogen; sodium hydride; potassium carbonate; potassium iodide; sodium hydroxide;
palladium on activated charcoal;
In
methanol; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid; water; sodium nitrite / 0 - 5 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h
3.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol / 1 h / 20 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 17 h / 120 °C
5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C
5.2: 0.17 h / 20 °C
6.1: water; sodium hydroxide / ethanol / 1 h / 60 °C
With
hydrogenchloride; sulfuric acid; water; hydrogen; sodium hydride; potassium carbonate; potassium iodide; sodium hydroxide; sodium nitrite;
palladium on activated charcoal;
In
methanol; ethanol; N,N-dimethyl-formamide;
