benzyl 3-methylglutarate

Base Information

Chemical Name:benzyl 3-methylglutarate
CAS No.:1360140-47-1
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:benzyl 3-methylglutarate

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Chemical Property of benzyl 3-methylglutarate

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Technology Process of benzyl 3-methylglutarate

There total 2 articles about benzyl 3-methylglutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4166-53-4
3-methylglutaric anhydride

: 100-51-6,185532-71-2
benzyl alcohol

: 1360140-47-1
benzyl 3-methylglutarate

Guidance literature:: With [Ni₂((R)-(C₁₀H₆NCHC₆H₃(O)2)2)]; In chloroform; at 0 ℃; for 48h; optical yield given as %ee; enantioselective reaction;
DOI:10.1021/ol3002078

Reference yield:

: 4166-53-4
3-methylglutaric anhydride

: 100-51-6,185532-71-2
benzyl alcohol

: 1402050-33-2
(R)-5-(benzyloxy)-3-methyl-5-oxopentanoic acid

: 1360140-47-1
benzyl 3-methylglutarate

Guidance literature:: With (1R,2R)-N,N-dimethyl-N'-[3,5-bis(trifluoromethyl)benzenesulfonyl]-1,2-diphenyl-1,2-ethanediamine; In diethyl ether; at 20 ℃; for 20h; optical yield given as %ee; enantioselective reaction;
DOI:10.1055/s-0029-1218374