Technology Process of C35H42N2O6Si
There total 11 articles about C35H42N2O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at -78 - 25 ℃;
for 1h;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1H-imidazole; sodium hydride / tetrahydrofuran; mineral oil / 0 - 25 °C
1.2: 1 h / 0 - 25 °C
1.3: 1 h / 0 - 25 °C
2.1: toluene / 36 h / 150 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
3.2: 2.5 h / -78 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
With
1H-imidazole; sodium hydride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/ja500548e
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
1.2: 2.5 h / -78 °C
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C
With
3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja500548e