bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

Base Information

Chemical Name:bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc
CAS No.:1401439-39-1
Molecular Formula:C₆₆H₆₈N₂O₂Zn
Molecular Weight:986.668
Hs Code.:

Synonyms:bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

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Chemical Property of bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

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Technology Process of bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

There total 2 articles about bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.1%

: 1401439-34-6
2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-methylphenol

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1401439-39-1
bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

Guidance literature:: 2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-methylphenol; With potassium hydride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

zinc(II) chloride; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.ica.2012.03.046

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 3-benzhydryl-2-hydroxy-5-methylbenzaldehyde

: 1401439-39-1
bis((2-((2,6-diisopropylphenylimino)methyl)-6-benzhydryl-4-ethyl)phenoxy)zinc

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / ethanol / 3 h / Inert atmosphere; Reflux

2.1: potassium hydride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

With potassium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol;
DOI:10.1016/j.ica.2012.03.046