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Technology Process of (C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4

(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4

Base Information
  • Chemical Name:(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4
  • CAS No.:510775-99-2
  • Molecular Formula:C32H12BF24*C39H47N2Ni
  • Molecular Weight:1465.73
  • Hs Code.:
(C<sub>10</sub>H<sub>6</sub>C<sub>2</sub>(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)Ni(CH(CH<sub>3</sub>)2)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4<sup>(1-)</sup>=((C<sub>10</sub>H<sub>6</sub>C<sub>2</sub>(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)Ni(CH(CH<sub>3</sub>)2))B(C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4

Synonyms:(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4

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Chemical Property of (C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4
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Technology Process of (C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4

There total 1 articles about (C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

Brookhart's acid

Brookhart's acid

(C<sub>10</sub>H<sub>6</sub>C<sub>2</sub>(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)Ni(CH<sub>2</sub>CH<sub>2</sub>CH<sub>3</sub>)2
510775-71-0

(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH2CH2CH3)2

(C<sub>10</sub>H<sub>6</sub>C<sub>2</sub>(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)Ni(CH(CH<sub>3</sub>)2)<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4<sup>(1-)</sup>=((C<sub>10</sub>H<sub>6</sub>C<sub>2</sub>(NC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2)2)Ni(CH(CH<sub>3</sub>)2))B(C<sub>6</sub>H<sub>3</sub>(CF<sub>3</sub>)2)4
510775-99-2

(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2)(1+)*B(C6H3(CF3)2)4(1-)=((C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH(CH3)2))B(C6H3(CF3)2)4

Guidance literature:
In dichloromethane; byproducts: propane; CH2Cl2 was added to a mixt. of Ni-complex and the oxonium acid at -80°C under Ar, soln. was stirred at -80°C for 30 min, allowed to warm slowly to -20°C; evapd. at -20°C, residue was dried in vacuo at 0°C for 2 hand stored at -35°C; low-temp. (1)H NMR and (1)H-(1)H COSY NMR;
DOI:10.1021/ja021071w
upstream raw materials:

(C10H6C2(NC6H3(CH(CH3)2)2)2)Ni(CH2CH2CH3)2

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