2-nitrobenzyl bromoacetate

Base Information

• Chemical Name: 2-nitrobenzyl bromoacetate
• CAS No.: 159538-04-2
• Molecular Formula: C₉H₈BrNO₄
• Molecular Weight: 274.071

Synonyms:2-nitrobenzyl bromoacetate

Chemical Property of 2-nitrobenzyl bromoacetate

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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MSDS Files:

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Technology Process of 2-nitrobenzyl bromoacetate

There total 2 articles about 2-nitrobenzyl bromoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2-Nitrobenzyl alcohol (612-25-9) + bromoacetic acid (79-08-3) → 2-nitrobenzyl bromoacetate (159538-04-2)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 120 ℃; for 24h;

DOI:10.1021/bm400221r

Reference yield:

2-Nitrobenzyl alcohol (612-25-9) + 2-Bromoacetyl bromide (598-21-0) → 2-nitrobenzyl bromoacetate (159538-04-2)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/acs.orglett.6b00981

Reference yield: 90.0%

2-(dimethylamino)ethyl methacrylate (2867-47-2) + 2-nitrobenzyl bromoacetate (159538-04-2) → C17H23N2O6(1+)*Br(1-) (1429483-13-5)

Guidance literature:

With hydroquinone; In acetonitrile; at 60 ℃; for 18h;

DOI:10.1021/bm400221r

upstream raw materials:

2-Nitrobenzyl alcohol

bromoacetic acid

2-Bromoacetyl bromide

Downstream raw materials:

C₁₇H₂₃N₂O₆⁽¹⁺⁾*Br^(1-)

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