benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

Base Information

Chemical Name:benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide
CAS No.:1204431-76-4
Molecular Formula:C₃₁H₂₈N₂O₇S
Molecular Weight:572.639
Hs Code.:

Synonyms:benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

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Chemical Property of benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

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Technology Process of benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

There total 2 articles about benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1204431-75-3
benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate

: 1204431-76-4
benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/ja104092z

Reference yield: 65.0%

: 1204431-76-4
benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

Guidance literature:

Reference yield: 70.0%

: 1204431-76-4
benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide

: 1204431-77-5
benzhydryl 6Z-[4'-carboxy-α-pyridylmethylidene]penicillinate-1,1-dioxide

Guidance literature:: benzhydryl 6Z-[4'-(allyloxycarbonyl)-α-pyridylmethylidene]penicillinate-1,1-dioxide; With sodium 4-methylbenzenesulfinate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; at 20 ℃; for 1h;

With hydrogenchloride; In water; ethyl acetate;